Extraction of plasticizers: An entire and reproducible
After each extraction step, resulting extract was analysed by GCMS for remaining plasticizers. This was considered to be important for a reliable quantitative analysis. The analysis was performed by a Shimadzu GCMS-QP2025 with direct inlet and a DB5 column (30 m x 0.25 mm x 25 μm).
Accelerated Solvent Extraction of Plasticizers from Polyvinyl
solvent extraction or Soxhlet conditions described above. AN70640_E 07/13S Application Note 336 Method Validation When developing extraction methods, one way to validate extraction efficiency is to re-extract the same sample and check for remaining analytes. The Dionex ASE system allows the analyst to automate re-extraction for easy method
The Latest Supply Chain Disruption: Plastics
Most supply chain practitioners would agree: between the pandemic, container shortages, winter weather, factory fires, the blocking of the Suez Canal by a container ship, and other logistics woes
Analytical methods for the determination of DEHP plasticizer
In the study by Wang et al., the simple room temperature extraction using chloroform was found to be the most efficient method for extracting alternative plasticizers like DEHA [42]. Polymer dissolution is also a solid–liquid extraction procedure that may be used to extract alternative plasticizers from medical device samples. The whole
US6223449B1 - Apparatus for extracting plasticizer - Google
The apparatus described in FIG. 2 is utilized to extract plasticizer from composite separator electrodes containing plasticizer. As with the extraction described in Example 1, the decreased chamber pressure facilitates evaporation at a lower temperature than would be possible at normal atmospheric pressure.
- How are plasticizers extracted from PVC?
- Plasticizers may account for 30–35% of the PVC formulation. Extraction and determination of plasticizers in PVC material are critical steps in evaluating a polymer for an intended use. Traditionally, plasticizers are extracted from PVC using a 6-h Soxhlet method and identified using infrared spectrometry or gas chromatography.
- What is a plasticizer in PVC?
- Plasticizers soften the polymer, aid in the manufacturing process, and provide form and function to various PVC materials. Plasticizers may account for 30–35% of the PVC formulation. Extraction and determination of plasticizers in PVC material are critical steps in evaluating a polymer for an intended use.
- How are PVC samples extracted?
- PVC samples were extracted using a 6-h Soxhlet extraction method (ASTM D 2124) and the accelerated solvent extraction method described above. Both methods used petroleum ether as the extraction solvent. Each extract was thoroughly dried, reconstituted using methy-lene chloride, and analyzed using the GC method described above.