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Method 606: Phthalate Ester - US EPA
required in order to reduce background phthalate levels to an acceptable level: 1) Heat four hours at 400°C in a shallow tray, 2) Heat 16 hours at 450-500°C in a shallow tray, 3) Soxhlet extract with methylene chloride for 48 hours. 6.5 Florisil—PR grade (60/100 mesh). Purchase activated at 1250°F and store in the dark in
